Details syllabus of fourth year ( 7th & 8th semester )

 

CEP 411 CORROSION ENGINEERING

2 Hours/Week, 2 Credits

Corrosion : general, electrochemical corrosion of metals , galvanic cells, corrosion rates (kinetics), types of corrosion with properties and phenomenon,  oxidation metals. Corrosion Testing: importance, classification materials and specimens , surface preparation , measuring and weighing, exposure techniques, duration, planned interval tests. Corrosion Prevention : Material selection, modification of metal, alternate of environment, design , cathodic and anodic protection, coatings (metallic ,inorganic ,non metallic and organic). Corrosion in Industries : Boiler plant, Double pipe heat exchangers, Shell and tub heat exchangers, Distillation Column

Books Recommended:

1. Fontana. G.,                          Corrosion Engineering

2. Uligue,                                  Introduction to Corrosion Engineering and its prevention

2. Banergy S. N.,                        Corrosion Engineering

 

CEP 412 PROCESS CONTROL

3 Hours/Week, 3 Credits

Laplace Transforms, transfer, functions for first order systems, physical examples of first order systems, response of first order systems in series, higher order systems, transportation lag. closed loop systems, controllers and final control/ elements, block diagrams, closed loop transfer functions, transient response of simple control systems, concepts of stability, stability craters, Routh test for stability.

Frequency response methods, control systems design by frequency response, closed loop frequency by frequency response methods, Nyquist stability criterion. Controller mechanism, measuring instruments, transducers and transmitters. Control of complex processes, experimental dynamics of complex processes. theoretical analysis of complex processes.

 

Books Recommended:

1. Hougen and Watson,                     Chemical  Process Principles I  & II 

2. Levenspiel,                                   Chemical reaction  engineering.

3.George Stephanopolos,                    Chemical process control

4.Donald R.Coughanowr,                     Process System Analysis and Control

 

CEP 414 Process Design

3 Hours/Week, 3 Credits

Introduction to process design, preliminary analysis & evaluation of processes, overview of flow sheet synthesis, mass & energy balances, equipment sizing & costing, economic evaluation, design & scheduling Of batch processes, analysis with rigorous process models, unit equation models, general concept of simulation for process design, process flowsheet optimization, basic concepts in process synthesis, heat and power integration, ideal distillation systems ,heat integrated distillation processes, geometric techniques for the synthesis of reactor networks, separating azeotropic mixtures , optimization approaches to process synthesis &design, basic concepts for algorithmic methods, synthesis of heat exchanger networks, synthesis of distillation sequences, simultaneous optimization & heat integration, optimization techniques for reactor network synthesis, structural optimization  of process flowsheets, process flexibility, optimal design scheduling for multi product batch plants. Conceptual Process Synthesis - Systematic hierarchical synthesis of flowsheets, Structural layers of a flowsheet. Reactor Network Synthesis - Reactor type and conditions for simple reaction systems, Use of attainable regional diagrams for complex reaction systems. Separation System Synthesis - Distillation column sequencing for ideal liquid      mixtures. Separation system structure for non-ideal mixtures using distillation /residue curves. Heat Exchanger Network Synthesis using Pinch Technology - Targets for minimum utilities, area, total cost. Maximum energy recovery design, Evolutionary synthesis for minimum number of exchangers design, Supertargetting, Heat and power      integration, Integration of heat exchanger network with distillation columns.

Books recommended:

1. Peters and Timerhaus,                     Plant Design and Economics for Chemical Engineers.

2. Douglas,                                        Conceptual Design of Chemical Process

3. Beigler, L. T.,                                 Systematic methods for chemical process design

4 Coulson & Richardson,                       Chemical Engineering. Vol-6

.

CEP 415 INDUSTRIAL ECONOMICS AND MANAGEMENT

2hours/Week, 2 Credits

 

Interest  and Investment cost: Simple interest, compound interest, continuous interest, applications of different types of interest, present worth & discount, Annuity, relation annuity and periodic payment, perpetuities and capitalized costs. Cost  estimation: Economic feasibility of project, capital investments, estimation of capital investment, cost indices, power factor, cost factors in capital investment, turn-over ratio, Types of taxes, insurances and insurance requirements for manufacturing concern. Depreciation: Types and methods of determining depreciation, depletion, evaluation of depreciation methods. Profitability analysis: GDP, GNP, Rate of return, payback period, pay out period, discounted cash flow, net present worth, Alternative investments, replacements.

Management: Management functions, Principles of management, Production management: Concept, scope and functions of production management, Production planning and control, continuous and intermittent products, Functions & scope of quality control, responsibilities of quality, Inspection, Zero defects. Marketing management: Concept, evolution, functions & importance of marketing, marketing mix. Financial management: Evolution, objectives & functions of financial management, financial analysis & control, Break-even analysis and profit planning, capital budgeting.

Motivation: Needs, theories of motivation (Maslow’s, Herzberg’s McGregor’s theories)

Optimizing techniques: Linear programming (Simplex and graphical methods)

Books recommended: 

1. Peters and Timerhaus,                  : Plant Design and Economics for Chemical Engineers.

2. Aurora,                                      : Industrial and Production management.

 

CEP416 MATHEMATICAL MODELING IN CHEMICAL ENGINEERING PROCESSES

2 Hours/Week, 2Credits

Introduction., classification of mathematical models, summary of model building processes, fundamental laws, fitting function of empirical data, factorial experimental designs & regression analysis, optimization methods, solution techniques for models, application to the problems: mass transfer, heat transfer, chemical reactor design, mathematical modeling for dynamic  and static behaviour of chemical processes.

 

Books recommended: 

1. T.F, Edgar, D.M. Himmelblau,               Optimization of Chemical Processes.

2. J. Miller,                                           Statistics for Advanced Models.

3.D.D.Joshi,                                           Linear Estimation & Design Of Experiments.

4.R,B.Bird, W.E, Stewart,                         Transport Phenomena.

5.G. Stephanopolas,                                 Chemical Process Control.

6.Luyben W. L.,                                       Process Modeling, Simulation & Control For Chemical Engineers,

 

CEP 417 CHEMICAL REACTION ENGINEERING SESSIONAL

3Hours/Week, 1.5 Credits

Laboratory classes based on Chemical Reaction Engineering Courses

 

CEP 418 PROJECT DESIGN

4 Hours/Week, 2 Credits

Students should design a chemical plant (INCLUDES ALL TYPE OF EQUIPMENT) independently based on the course no. CEP 414.

 

CEP 419 INPLANT TRAINING

1.5 Credits

Industrial visits and training.

 

CEP 420 TRANSPORT  PHENOMENA

3 Hours/Week, 3 Credits

 Viscosity and the Mechanism of Momentum Transport, Newton’s Law of Viscosity, Non-Newtonian Fluids, Pressure and Temperature Dependence of Viscosity, Theory of Viscosity of Gases at low Density, Theory of Viscosity of liquids. velocity Distributions in laminar flow , Shell Momentum Balances: Boundary Condition, Flow  of a Falling Fill, Flow through a Circular Tube, Flow through an Annulus ,Adjacent Flow of Two Immiscible Flow , Creeping Flow Around a Solid Sphere, The Equations of Change for Isothermal Systems.   The Equation of Continuity, The Equation of Motion, The Equation of Mechanical Energy, The Equation of Change in Curvilinear Coordinates, Use of the equations of change to set Up Steady flow Problems, The equations of change for Incompressible Non-Newtonian Flow, Dimensional Analysis of the Equations of Change Velocity Distributions with More Than One Independent Variable Unsteady Viscous Flow, Steady Viscous Flow With Two Nonvanishing Velocity Components: The stream Function, Steady two-dimensional Potential Flow Boundary-Layer Theory, Energy Transport. Thermal Conductivity and the Mechanism of Energy Transport Fourier’s Law of Heat Conduction, Temperature and Pressure Dependence of Thermal Conductivity in Gases and Liquids, Theory of Thermal Conductivity of Gases at Low Density, theory of thermal conductivity of liquids, thermal conductivity of solids. Temperature Distributions in solids and in Laminar Flow: shell energy balances boundary conditions, heat condition with an electrical heat source, heat conduction with a nuclear heat source, heat conduction with a viscous heat source, heat conduction through composite walls: addition of resistance, heat conduction in a cooling fin. The equations of change for nonisothermal systems: the equation of energy, the energy equation in curvilinear coordinates, the equations of motion for forced and free convection in nonisothermal flow, summary of the equations of change, use of the equations of change to set up steady-state heat transfer problems. Temperature distributions with more than one independent variable: unsteady heat conduction in solids, steady heat conduction in laminar flow of a viscous fluid, steady two-dimensional potential flow of heat in solids, boundary layer theory.

 

Book Recommended

 1. Bird. R, .B,.                       :Transport Phenomena,   Wiley Inter Science Singapore

 

CEP 421 ENVIRONMENTAL ENGINEERING

3 Hours/Week, 3 Credits

Pollution of the environment: a) Air pollution: composition and evaluation of the atmosphere; Earth’s radiation balance; particles, ions and radicals in the atmosphere, chemical and photochemical reactions, depletion of the ozone layer, green house effect. Air pollutants and their effects. Water pollution: water resources. the hydrologic cycle, complexation in natural water and waste water, micro organisms-catalysts of aquatic chemical reaction, eutrofication, water pollutants inorganic, organic sediments, radioactive materials. Water pollution control processes: Study of physical and biological processes employed for pollution control, removal of suspended, colloidal and dissolved phases of pollution. Industrial wastes: Waste water treatment, Study of unit operation and processes ,sludge handling and disposal effects, disposal of waste waters in ground water s travel of pollutants through soil, removal of nutrients and pollutants by soil interaction Solid wastes, sources, municipal refuse, industrial solid wastes, contamination by basic organic chemicals and toxic metals, comparative treatment of incineration, chemical treatment, solidification encapsulation and land-fill. Environmental problems in Bangladesh: environmental degradation from industries. factories, agricultural fields and domestic wastes and disposal, weather change, water supply and sanitation legislation in Bangladesh as applied to poisonous and special wastes.

 

Books Recommended:

1. W. Strauss,                       Air pollution.

2. A.S.Stoker,                        Air and Water pollution

3. Bailey and Clark,              Chemistry of the Environment.

4. J.N. Duffus,                       Environmental Toxicology.

 

CEP 422 NATURAL GAS AND PETROLEUM RESERVOIR ENGINEERING.

3 Hours/Week, 3 Credits

Natural Gas Technology and Earth Sciences: Branches of Petroleum Industry. Sources of Information for natural gas engineering and its applications. Geology and earth sciences: Earth sciences-Historical geology, Sedimentation process, Petroleum reservoirs, Origin of petroleum. Earth temperatures & pressure, Earth temperatures, Earth pressures. Petroleum : Natural gas, LP gas, Condensate, & Crude oil. Properties of rocks: Types of rocks. Porosity, Permeability: Measurement of permeability. Drilling and completion of wells: Processing in drilling, Stimulation of well productivity, Gas fracturing, Acidizing operations, Well logging, Open hole logging, Cased hole logs. FLOW IN RESERVOIR &ADJACENT AQUIFER: Pressure drop from reservoir to wellbore -A simplified steady state approach. Basic fluid flow equations-General flow equation in dimensionless forms, Boundary conditions. Partial penetrated wells, Superposition principle,  Water influx at gas reservoir Edge -  Constant terminal flow rate case,  Constant terminal pressure case, Practical considerations, Continuation of materials balance with movement equations, The moving boundary problem. GAS WELL-TESTING:  Deliverability tests- Back pressure test, Isochronal test, Modified isochronal test, Inverse productivity index. Test for determining reservoir parameters-drawdown test, multi-Rate test, Two-Rate test, Build up test, Determination of equalized reservoir pressures, Type-curve method. RESERVOIR  ENGINEERING APPLIED TO GAS, GAS/CONDENSATE & GAS/OIL FIELDS: Solubility & shrinkage (PVT) curves, Predicting solubility & formation volume factors (FVF), Oil & gas reserves- volumetric method, Material  balances, Recoverable gas. Variations in behavior, Mechanism of oil recovery from reservoirs, Oil recovery predictions- Gas/ Condensate reservoirs, Processing Condensate well Fluids, Vapor liquid equilibria applied to reservoirs, Recovery of revaporized condensate in gas storage.

Books Recommended:

 1.  Katz D. L. et al., Natural Gas Engineering (production & storage), McGraw-Hill, Singapore

 

CEP 423 POLYMERS IN APPLICATION:

3 Hours/Week, 3 Credits

 Commercial polymers: Polymerization techniques, properties, and application of polyethylene, polypropylene, polyvinyl chloride, polystyrene, polyamide, polyesters, UF-resin, MF-resin, PF-resin, polyurethanes, epoxy resin, polycarbonates, silicon polymer. Natural rubbers: properties of rubber, latex, preservation of latex, rubber plants, and rubber vulcanization. Synthetic rubbers:  Buna S, Buna N, Neoprene rubber, Thiokol, Butyl rubber, urethane rubber.

Polymer blends: Definition and classification of polymer blends, thermodynamics of polymer blends, spinodal and bimodal curve, application of polymer blends.

Polymer Composites:  Introduction, fiber reinforced composite, predicting properties of fiber reinforced composite, characteristics of fiber reinforced composite, mfg. of fiber and composite Glass fiber reinforced plastics.

Polymer alloys

 

CEP 427* ADVANCED CHEMICAL ENGINEERING SESSIONAL

1.5 credits, 3 hr/ week                                 Various types of Industrial project design.

 

CEP 428* ADVANCED POLYMER SC. AND ENGG SESSIONAL

1.5 credits, 3 hr/ week                Various types of Industrial project design such as Industrial Polymer Reactor and Process Design.

 

CEP 429* THESIS

3 credits

CEP 431* Project

3 credits

 

CEP 430 ORAL

1.0credit

 

ELECTIVES

(Courses would be offered as per availability of respective teachers)

 

CEP 432 PETROLEUM REFINERY ENGINEERING

2 Hours/Week, 2 Credits

 

Origin Formation and Compositon of Petroleum: origin and formation of petroleum ,reserves and deposits of world ,composition of petroleum. Petroleum Processing Data: evaluation of petroleum ,thermal properties of petroleum, fractions , important product properties and test methods. Fractionation of Petroleum :dehydration and desalting of crudes ,heating of crude-pipe still heaters, distillation of petroleum, blending of gasoline. Treatment Techniques: fraction-impurities ,treatment of gasoline, treatment of kerosene, treatment of lubes, wax and purification. Thermal and Catalytical Process: cracking, catalytic cracking, catalytic reforming, naphtha cracking, cooking, hydrogen processes, alkylation processes isomerisation processes polymer gasolines. Asphalt Technology :source of asphalt , air blowing of bitumen, upgradation of heavy , crudes.

 

Book Reference.

 1. B.K. Bhaskara Rao                        Modern Petroleum  Refining Process.

2. G.N. Sarkar.                                     Petroleum Refining

 

CEP 433 CHEMICAL ENGINEERING PRINCIPLES IN PAPER TECHNOLOGY

 2 Hours/Week, 2 Credits

Principles of paper making technology - Application of Chemical Engineering Principles to Pulp and Paper industry; Wood - Selection, types, comparison with other raw materials. Pulping - Process, including mechanical and Kraft pulping, bleaching, soda cycle      for effluents

Paper Machine - Principles of forming paper, steam drying and its effects. Coating and Finishing - Different coating principles, blade, rod metering etc. and supercalendering. Effluent Treatment - How the different waste water streams from each of these operations is treated.

 

References:

1. Shreves Chemical Process Industry, George T. Austin (V Edn.) 1997, McGraw      Hill

2. Paper Basics by David Saltman, Van Nostrand, 1978.

 

CEP 434 INTRODUCTION TO COMPUTER CONTROL OF PROCESSES

2 Hours/Week, 2 Credits

 

Introduction to Hardware Elements - Analog to digital and digital to analog       converters, sample and hold circuit.       Introduction to distributed digital control system architecture.       Digital Signal Conditioning - Sampling of continuous systems, Shannon's sampling       theorem, Practical guidelines for selection of sampling period, Signal reconstruction       with sample and hold, Digital filters.        z-Transforms - z-transforms, Properties of z-transforms, Inverse z-transforms,      Solution of difference equation using z-transforms.

Pulse Transfer Function - Development of pulse transfer function from Laplace      transfer function, Development of linear discrete state space model from nonlinear       first principles model, Development of pulse transfer function from discrete state      space model.       System Identification - Identification of system parameters from input-output data,       Statistical interpretation of least squares, Recursive least square estimation,

Selection of perturbation signal for model identification.

Closed Loop Transfer Function - development of closed loop transfer function,

Effect of disturbances on closed loop. Stability Analysis - derivation of stability criteria for transfer function and state space models, Jury's stability test, Controllability and observability.  Classical Control Algorithms - Velocity form of PID controller, Dalhin's controller, State and output deadbeat controller, Vogel-edgar controller, Morari-Zafiriou algorithm, Internal model controller.

Modern Control Algorithms - Regulator and state observer design using pole placement (Ackermann's formulae), Separation principle. 

Introduction to model predictive control and adaptive control schemes.

 

References:

1. E. Seborg, J.F. Edgar and D.A. Mellichamp,          "Process Dynamics & Control",

John Wiley 1989.

2. K.J. Astron and B. Wittenmark,                      "Computer Controlled Systems", Prentice - Hall, 1994.

 

CEP435 RENEWABLE ENERGY

2 Hours/Week, 2 Credits

 

Potential for renewable energy sources, energy conservation, Solar Energy - thermal and photoelectrical - Ocean thermal energy sources - Geothermal energy       utilization - Wind energy - Bio-gas principles, reactors. Hydrogen source of       energy, Solar and Chemical production of hydrogen, Metal Hydrides, Microhydel

systems, Hybrid systems, Heat pump applications in process engineering.      

References:

1. J. Twidell and T. Weir, Renewable energy sources, Cambridge University Press,

      1986.

2. S.P. Sukhatme, Solar energy, 2nd Ed., Tata McGraw Hill, 1996.

3. T. Ohta, Solar - hydrogen energy system, Pergamon Press, 1979.

 

CEP 436 ADVANCED MOMENTUM TRANSFER

2 Hours/Week, 2 Credits

 

Reynolds transport theorem, Conservation equations for mass, momentum, energy and a passive scalar. Some exact solutions to Navier-Stokes equations, `Creeping flow, Drag, Boundary       layer theory.        Flow separation.       Laminar flow, Transition to turbulence, Turbulent flow, Reynolds stresses, Eddy       viscosity, mixing length theory, Flow over a flat plate, Universal velocity profile.

Flow through conduits, Roughness, Empirical correlations for friction factor in straight pipes, Pressure losses due to pipe fittings, Pipes in series and in parallel. Non-Newtonian fluids, Constitutive equations, Viscoelasticity.       Applications, Flow through porous media, Fluidizations, Multi-phase flow.

 

References:  1. R.B. Bird, W.E. Stewart and E.N. Lightfoot, "Transport Phenomena", Wiley International Edition, 1960

CEP437 POLYMER KINETIC THEORY

2 Hours/Week, 2 Credits

 

Flow Phenomena in Polymeric Liquids.

The chemical nature of polymeric liquids; Non-Newtonian viscosity, Normal stress. effects, other elastic effects; Material functions for Polymeric liquids, shear and      shear free flows. Basic Concepts from Probability Theory; Events and probabilities; Random variables; Expectations and moments; Joint distributions and independence; Gaussian random variables; General discussion of the random walk ; Fokker- Planck equations

References :

1. R.B. Bird, C.F. Curtiss, R.C. Armstrong and O. Hassager, Dynamics of

polymeric liquids, Volume 2: Kinetic theory, 2nd Ed., John Wiley

 

CEE 405 ENVIRONMENTAL MANAGEMENT AND AUDITING

2 Hours/Week, 2 Credits

 

CEP 438 INDUSTRIAL LECTURES

2 Hours/Week, 2 Credits

 

CEP 439 HAZARD ASSESSMENT AND MITIGATION IN CHEMICAL PROCESS INDUSTRIES

2 Hours/Week, 2 Credits

 

Hazards and Safety in Chemical Industries - Introduction to risk management, Principles and issues in risk analysis, Acts and regulations. Hazard Management - Quantitative risk assessment, Hazard identification, Hazard and operability studies. Hazard Analysis - Event tree and fault tree analysis frequency analysis,

Consequence analysis. Data sources and data selection. 

Risk criteria and cost benefit analysis, Safety audit and safety regulations.

Elements of emergency planning and preparation of disaster management plan,

Case studies of chemical disasters.

 

References:

1. F. Lees, "Loss Prevention in the Process Industries", Butterworth Heinman,

      1995.

2. J.J. Mewis, H.J. Pasman and E.E. Rademacker - Eds., "Loss prevention and

      Safety Promotion in the Processing Industries, Proc. Of 8th International

      Symposium", Antwerp, Belgium, Elsevier, 1995.

3. W. Hallenback and K.M. Cunnishem, "Quantitative Risk Assessment for

      Environmental and Occupational Health", Lewis Pub., 1986.

 

 CEP 440 PRINCIPLES OF CATALYSIS

2 Hours/Week, 2 Credits

 

Catalysis in Solutions: Introduction, acid-base, catalysis in the gas phase, catalysis in dilute aqueous solution  general and specific acid and base catalysis, catalysis in concentrated strong acid solutions, catalysis by bases, stepwise and concerted reactions, catalysis by metal ions, hydrocarbon conversion. Catalysis by Polymers: the nature of polymers, attachment of catalytic groups to polymer supports, catalysis in polymer gels, adsorption and the kinetics of polymer-catalyzed reactions, interactions of catalytic groups, the role of the support, bifunctional and multifunctional catalysis. Catalysis on Surfaces: Introduction, adsorption, adsorption isotherms, structure of adsorbed species on single crystal metal surfaces, adsorption on complex surfaces, functionalied surfaces, olefin polymerization catalysis on titanium trichloride surfaces, catalysis on metal surfaces, catalysis on metal oxide surfaces, catalysis by supported metals, catalysis by metal sulphides

 

CEP 101 PROCESS TECHNOLOGY (For IPE) 

2 hours / week, 2 credit

Pulp and Paper Industries: Raw materials, mfg. of different types of pulp paper boards, black lacquer recovery, deinking of waste paper, pulp and paper industries in Bangladesh. Soap and Detergent Industries: Raw materials, mfg. of different types of soap, recovery of the glycerin, classification of the detergents, industrial processing for the alkyl  aryl sulphonates (AAS), environmental pollution by detergents. Biodegradability of detergents. Introduction of  chemical fertilizer: Nitrogenous fertilizer : Raw materials of ammonia production of synthesis gas in ammonia plants, technology of urea manufacturing; Process used in Urea industries of Bangladesh . Cement industries: Composition, properties and uses different types of cements, manufacture of cement by different methods, setting and hardening of cement, testing of cement. Lubricants: Various types of lubricants, Production of lubricants, Properties of Various types of lubricants.

 

Books Recommended:

1.  G.N  Pandey,                     A Text Book of Chemical Technology Vol. I and II

2.  N. Austin                          Chemical Process Industries.

4. Anderson and Winzet,         Introduction to Chemical Engineering

5. Riegl’s,                              Industrial Chemistry

6. B. K. Sharma,                    Industrial Chemistry

7. S.S. Dara,                        A text book of Engineering Chemistry.

 

CEP 301 COMPOSITE MATERIALS

2 cr, 2 hr/week

Introduction: The natural composite wood, Jute and Glass Fibers. Modification of Natural Fiber, Jute-polymer composite, fabrication of composite. Properties of composite: Particulate-Reinforced composite Materials, Dispersion-Strengthened composite, True particulate composite, Fiber-reinforced composites, Predicting properties of fiber-reinforced composite, Characteristics of fiber-Reinforced composites, Manufacturing fiber and composites, Fiber reinforced systems, Laminar composite materials. Thermoplastics composite materials: matrix resins, Reinforced fibers, interfaces and interphases; application. Future development: new composites, design strategies, process technology, resource managements, and added function. Thermal and photo-degradation behavior of glass fiber.

 

Book Recommended:

1.    F. N. Cogswell,                       “Thermoplastic Aromatic Polymer Composites”

2.   Donald. R. Askeland,                “The Science & Engineering of Materials”

3. Lawrence H. Van. Vlack,             “Elements of Material Science and Engineering”

4. George S. Springer,                    “Envirinmental Effects on composite Materials, Vol-2”

 

CEP 401 ELEMENTS OF CHEMICAL ENGINEERING AND TECHNIQUES OF ENVIRONMENTAL ANALYSES (for CEE)

2 Hours/Week ,2 Credits

 

Mechanical separation; gravity settlers, impingement separators; centrifugal separators and scrubbers.  Crushing and grinding : solid handling machinery, Fluid moving machinery, ejectors and vacuum systems, pressure relieving devices, Mixing and agitation, Crystallization, drying and evaporation. Scope of chemical engineering, Principles of chemical engineering calculations, system of units, basic concepts of dimensional analysis, process variables, basis of calculation , conversion of mass and energy material balance, overall component balance, recycle and bypass, simple reactive systems and combustion reactions, Energy balance, forms of energy and first law of thermodynamics, thermodynamics data and tables, energy balances on open closed systems. Application of mass and energy balance to real process,  Measurement of process variables; fluid static's and manometer, temperature measurement and flow measurement.

1. Introduction to instrumental analysis; introduction to analytical spectrometry; absorption laws; spectral interfaces,

2. UV-VIS spectroscopy; introduction, electronic transitions, instrumentation, qualitative and quantitative analysis.

3. Atomic spectroscopy : (a) Frame emission spectroscopy. (b) Atomic absorption spectroscopy. (c) Inductively coupled plasma emission spectroscopy.

4. X- ray spectroscopy : Introduction, general theory and instrumentation. X-ray absorption and emission methods.  X-ray diffraction methods; X-ray flume scheme.

5. Neutron activation analysis: Anionic stripping voltametry.

6. Chromatography : Principles and classification of chromatographic techniques; paper chromatography TLC; column chromatography; Gas chromatography, high performance liquid chromatography. 

 

Books Recommended:

1.Geankopolise-                                 Unit Operation

2.Mc Cabe and Smith,                          Unit Operation of Chemical Engineering

3. Faoust,  A. S.,                                Principles of Unit Operations.

4. Coulson and Rechardson                   Chemical Engineering

5. B. Christian,                                   Analytical chemistry.

CEP 402 ENVIRONMENTAL ANALYSIS (FOR CEE)

2 Hours/Week, 1 Credit

 

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